63种农药混标溶液 WQ-4 (168-26011)

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63种农药混标溶液 WQ-4

货号：168-26011
包装：1ml

  • 英文名：63 Pesticides Mixture Standard Solution WQ-4 (each 20μg/ml Acetonitrile Solution)
  • 级别：农药残留分析
  • 品牌：Wako

    • 63种农药混标溶液 WQ-4（每种20μg/ml乙腈溶液）wako#168-26011，用于农药残留分析。

    产品详情质检信息

    63种农药混标溶液 WQ-4（每种20μg/ml乙腈溶液）

    63种农药混标溶液 WQ-4（每种20μg/ml乙腈溶液）wako#168-26011，用于农药残留分析。
    生产厂商：富士-和光化学纯药株式会社
    储存条件：-20°C
    GHS: Danger
    外观：淡黄色澄清液体。
    Oxamyl, Nitenpyram, Pymetrozine, Monocrotophos, Imidacloprid, Cinosulfuron, Acetamiprid, Thiacloprid, Pyrazosulfuron-ethyl, Cyanazine, Ethoxysulfuron, Fluazifop, (E)-Metominostrobin, Linuron, Acibenzolar-S-methyl, Ametryn, Boscalid, Cumyluron, Benzobicyclon, Prometryn, Diclomezine, Chromafenozide, Simeconazole, Tetraconazole, Naproanilide, Tebuconazole, Pirimiphos-methyl, Triflumizole, Benzofenap, Quizalofop-ethyl, Dinotefuran, Thiamethoxam, Clothianidin, Trinexapac-ethyl, Metribuzin, Bromacil, Bendiocarb, Furametpyr, Cyproconazole, Indanofan, Diflubenzuron, Tetrachlorvinphos (CVMP), Cyprodinil, Fentrazamide, Etobenzanid, Oxadiargyl, Phoxim, Pyrazolynate (Pyrazolate), Difenoconazole, Oxaziclomefone, Pentoxazone, Clomeprop, Silafluofen, MCPA (MCP), Dichlorprop, Propanil (DCPA), Inabenfide, Tiadinil, Thifluzamide, Flusulfamide, Tebufenozide,Fluazinam : 每种19.4 – 20.6ug/ml
    (Z)-Pyriminobac-methyl, (E)-Pyriminobac-methyl : 每种 9.7 – 10.3ug/ml

    分析案例

    液相质谱图谱

    63种农药混标溶液 WQ-4 (168-26011)
    峰编号 组分 监测离子
    (m/z)    		 模式 峰编号 组分 监测离子
    (m/z)    		 模式 峰编号 组分 监测离子
    (m/z)    		 模式
    前体 产品 前体 产品 前体 产品
    1 Oxamyl 237 72 + 22 Simeconazole 294 70 + 43 Indanofan 341 175 +
    2 Pymetrozine 218 105 + 23 Naproanilide 292 171 + 44 Diflubenzuron 311 158 +
    3 Thiamethoxam 292 211 + 24 Tebufenozide 351 133 + 45 Tetrachlorvinphos
    (CVMP)    		 367 127 +
    4 Trinexapac-ethyl 253 69 + 25 Difenoconazole 406 251 + 46 Tebuconazole 308 70 +
    5 Cinosulfuron 414 183 + 26 Triflumizole 346 278 + 47 Cyprodinil 226 108 +
    6 Acetamiprid 223 126 + 27 Benzofenap 431 105 + 48 Fentrazamide 350 154 +
    7 Thiacloprid 253 126 + 28 Quizalofop-ethyl 373 299 + 49 Etobenzanid 340 179 +
    8 Pyrazosulfuron-ethyl 415 182 + 29 Oxaziclomefone 376 190 + 50 Oxadiargyl 358 341 +
    9 Cyanazine 241 214 + 30 Dinotefuran 203 129 + 51 Phoxim 299 77 +
    10 Bromacil 261 205 + 31 Nitenpyram 271 56 + 52 Pirimiphos-methyl 306 164 +
    11 Bendiocarb 224 167 + 32 Monocrotophos 224 193 + 53 Pyrazolate 439 91 +
    12 Ethoxysulfuron 399 261 + 33 Imidacloprid 256 209 + 54 Clomeprop 324 120 +
    13 Furametpyr 334 157 + 34 Clothianidin 250 132 + 55 Pentoxazone 371 286 +
    14 (E)-Metominostrobin 285 196 + 35 Metribuzin 215 49 + 56 Silafluofen 426 287 +
    15 (Z)-Pyriminobac-methyl*** 362 330 + 36 Fluazifop 328 282 + 57 MCPA(MCP) 199 141 –
    16 Ametryn 228 186 + 37 Linuron 249 182 + 58 Dichlorprop 233 161 –
    17 (E)-Pyriminobac-methyl*** 362 330 + 38 Acibenzolar-S-methyl 211 136 + 59 Propanil(DCPA) 216 160 –
    18 Cumyluron 303 185 + 39 Boscalid 343 307 + 60 Inabenfide 337 122 –
    19 Cyproconazole 292 70 + 40 Benzobicyclon 447 257 + 61 Tiadinil 266 71 –
    20 Prometryn 242 158 + 41 Diclomezine 255 141 + 62 Thifluzamide 527 125 –
    21 Chromafenozide 395 175 + 42 Tetraconazole 372 159 + 63 Flusulfamide 413 171 –
      64 Fluazinam 463 416 –
    * 该产品含2%甲醇。
    ** 分析条件，图标和检测离子仅供参考。不能当作农药混合标准溶液的确定数据使用。
    *** 制备溶液浓度，作为E和Z型异构体的总和，可转换成20 μg/mL(每种10 μg/mL)。
    检测条件
    【仪器】
    岛津 LCMS-8040
    【液相条件】
    柱子：Wakopak? Ultra C18-3　2.0 × 75 mm
    柱温：40 ℃
    洗脱液：A) 5 mmol/L甲酸铵水溶液；B) 5 mmol/L甲酸铵甲醇溶液
    梯度

    时间 (分钟) B 浓度(%)
    0-2 5
    2-6 5-40
    6-41 40-75
    41-45 75-100
    46-50 100
    50-50.01 100-5
    50.01-60 5

    流速：0.15 毫升/分钟

    【质谱条件】
    电离：ESI（电喷雾电离）
    模式：多反应检测扫描（MRM）

    产品列表

    产品编号 产品名称 产品级别 包装
    164-26013 63 Pesticides Mixture Standard Solution WQ-4 (each 20μg/ml Acetonitrile Solution)
    63种农药混标溶液 WQ-4（每种20μg/ml乙腈溶液）    		 农药残留分析 1mLx5A
    168-26011 1mL

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